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Using inert atmospheric control (Fuse 1+ 30W)

Using inert atmospheric control (Fuse 1+ 30W)

Note:

Check the support article Choosing the right powder to determine whether the powder you are using requires inert atmospheric control.

Inert atmospheric control is the process of removing air from an enclosed space by replacing it with an inert gas. In SLS 3D printing, the inert gas is typically nitrogen. SLS polymers tend to oxidize when held at elevated temperatures for extended periods of time. Limiting oxidation improves the material properties of printed parts and allows you to print with a lower refresh rate.

For example, printing with Nylon 11 in nitrogen allows you to use a 30% refresh rate to print parts with increased ductility compared to parts printed in air at a 50% refresh rate.

The Fuse 1+ 30W is equipped with a sealed chamber held at a partial positive pressure to ensure a low oxygen concentration when printing in an inert atmosphere. The Fuse 1+ 30W includes plumbing, sensors, and controls to enable a plug-and-play inert atmospheric control process. The Fuse 1+ 30W does not contain nitrogen generation capabilities, so an external nitrogen source is needed if inert atmospheric control is desired.

Sourcing

Nitrogen may be sourced in several forms including compressed gas cylinders, liquid nitrogen dewars, or nitrogen generators.

Nitrogen supplies that meet the following requirements are suitable for use with the Fuse 1+ 30W:

  • Concentration: 99.5% or greater
  • Flow: 0.5 SCFM or greater
  • Pressure range: 36–125 psi
  • Gas temperature at machine inlet: 18 °C or greater

For more information about sourcing supplies, read the support article Formlabs-approved distributors for supplies (SLS). The table below summarizes the trade-offs between options:

Nitrogen generatorCompressed gas cylinderLiquid nitrogen dewarMicro-bulk/bulk tank
Example imageExample of a nitrogen generatorExample of a compressed gas cylinderExample of a liquid nitrogen dewarExample of a bulk nitrogen tank
CapacityContinuousRoughly 300 SCF (8,495 L) of nitrogen or 10 hours of printing per cylinderRoughly 5,760 SCF (163,105 L) of nitrogen or 6–7 days of printing per 230 L dewar (with losses)Depends on installation type and capacity
Cost4,000–10,000 USD per generator80–120 USD per cylinder70–120 USD per dewar
Site requirements
  • Air compressor with treated air (dry and filtered)
  • Pneumatic tubes and fittings
  • Wall space to chain cylinders in place for safety
  • Pneumatic tubes and fittings
  • Loading dock access required for cylinder swaps
  • Sufficiently long tube to allow nitrogen gas to reach temperature requirements
  • Pneumatic tubes and fittings
  • Loading dock access required for dewar swaps
Dedicated installation: consult with vendors for site requirements
Other considerations
  • Low maintenance: no need to swap out cylinders
  • May have a longer lead time than compressed or liquid nitrogen options
  • Requires 2–2.5 SCFM of compressed air
  • Low initial setup cost and short lead time
  • Cylinders must be replaced when empty
  • Oxygen sensor recommended for safety
  • Low initial setup cost and short lead time
  • Dewars must be replaced when empty
  • Flow meter and oxygen sensor recommended for safety
Recommended vendors

Holtec Gas Systems (North America)
DWT (Europe)
Flairmo

AirgasAirgasAirgas

Nitrogen generators

Nitrogen generators convert a compressed air source into a flow of high-purity nitrogen gas, with most of the oxygen removed. The resulting flow of nitrogen can serve as a nitrogen source for the Fuse 1+ 30W. A primary benefit of using nitrogen generators is that they do not require replacing or refilling bottled nitrogen sources.

Air compressors may have a high startup power draw and should be powered by a separate circuit from the printer to prevent print interruption.

Formlabs recommends using a dedicated air compressor or one with sufficient capacity to prevent pressure drops if used by other devices during printing. Compressed air fed into a nitrogen generator must be filtered to remove moisture, oil, and particulate matter.

For recommended nitrogen generators and associated fittings, please see the Formlabs-approved distributors for supplies support article. The listed fittings are compatible with the recommended HSS-7 or HSS-3 model nitrogen generator from Holtec Gas Systems. The fittings include:

  1. Quick disconnect hose coupling for air (1x): Quick disconnect couplings allow for ease of setup. Note that smaller compressors typically use ¼” coupling size, but higher-capacity compressors may use larger couplings. Check your compressor to ensure compatible pipe size and coupling size.
  2. Quick disconnect hose socket for air (2x): Quick disconnect sockets allow the air hoses to interface easily with the air compressor and printer. The hose sockets are connected to the threaded ends of two separate air hoses.
  3. EPDM air hose (2x; 3x if used with an external compressed air filter): Compressed air hoses connect the air compressor to the nitrogen generator and the nitrogen generator to the printer’s nitrogen inlet. Three air hoses are necessary if you are using an external compressed air filter.
  4. Compressed air filter (1x, if applicable): Compressed air fed into a nitrogen generator must be filtered to remove moisture, oil, and particulate matter. If your air compressor is pre-equipped with a filter, you do not need an additional external filter. The filter must be in line prior to the nitrogen generator.
  5. Thread sealant tape: Use thread sealant tape to ensure an airtight connection on any threaded connections.
  6. Nitrogen generator: Formlabs has tested the HSS-7 nitrogen generator from Holtec Gas Systems. Any nitrogen generator that can supply the required nitrogen input requirements may also be used. If using other nitrogen generators, ensure that the couplings are compatible with your hoses and adapters as applicable.

The diagram below depicts how the components above are assembled to successfully provide nitrogen to the Fuse 1+ 30W, starting with an air compressor (not shown). Note that the items in the dashed box are not required if your air compressor is pre-equipped with a filter.

Fittings to supply a Fuse 1+ 30W via a nitrogen generator

The picture below shows the location of the nitrogen inlet on the Fuse 1+ 30W. Note that the included quick disconnect hose coupling is installed.

Nitrogen inlet on the Fuse 1+ 30W

Nitrogen bottles, dewars, and tanks

Nitrogen may also be supplied to the Fuse 1+ 30W from nitrogen containers such as compressed gas cylinders, liquid nitrogen dewars, or micro-bulk or bulk containers. The best option depends on printing volume, budget, and facilities. For a recommendation on your best option for nitrogen, use the Formlabs Gas Calculator developed by Airgas.

Nitrogen cylinders may serve as a low cost way to begin printing with an inert gas atmosphere without the need to invest in a compressor and nitrogen generator. Bulk supplies may also serve as a cost-effective option for high-volume printing in production environments.

When using compressed gas sources of nitrogen, install a regulator at the outlet of the compressed gas source in order to lower the nitrogen pressure to the input range of the Fuse 1+ 30W.

When using liquid nitrogen sources, install an evaporator at the outlet of the liquid nitrogen source in order to convert it to a gas which can be used as an input to the Fuse 1+ 30W.

Preparing the nitrogen system (Fuse 1+ 30W only)

The Fuse 1+ 30W has the option to use nitrogen as an inert gas atmosphere in the print chamber. The inert nitrogen atmosphere prevents the oxidation of plastic powder.

The Fuse 1+ 30W has two atmospheric control modes:

  • Air Mode: the print enclosure atmosphere is composed of atmospheric air
  • Nitrogen Mode: the print enclosure is purged with a supply of nitrogen gas

To prepare the Fuse 1+ 30W for printing with an inert gas atmosphere:

  1. Connect the nitrogen supply to the nitrogen interface at the rear of the printer.
  2. Confirm that nitrogen supply pressure into the Fuse 1+ 30W is between 248–862 kPa (36–125 psi) and the flow rate is at least 14 L/min (0.5 SCFM).
  3. When using a nitrogen supply such as bottled nitrogen gas or liquid nitrogen, ensure that there is enough available nitrogen to complete the print. When printing with an inert gas atmosphere, the printer requires approximately 14 L (0.5 cu ft) of nitrogen gas per minute.
  4. Tap the printer icon in the left sidebar to access the printer status screen. Toggle Nitrogen System to ON.
  5. Confirm that the touchscreen shows N2 Mode and that both the Inlet Pressure and the Valve Pressure are in range.

To adjust the valve pressure:

  1. Tap the printer icon in the left sidebar to access the printer status screen.
  2. Under Nitrogen System, tap Valve Pressure. The Nitrogen Setup window opens.
  1. Lift the IR sensor access door on the top of the printer. The nitrogen pressure knob is located to the left of the IR sensor.
  2. Slowly and carefully adjust the nitrogen pressure knob until the onscreen needle is in the highlighted zone.
  3. Wait for the reading to settle between each adjustment.
Fuse 1+ 30W nitrogen knob

Note:

The nitrogen pressure knob is extremely sensitive. If the onscreen needle is jumping between pressure readings, make smaller adjustments.

  1. When the nitrogen pressure is sufficiently adjusted, tap Done.
  2. Close the IR sensor access door.

Safety

Warning:

Ensure that proper ventilation is available to prevent health and safety issues associated with lack of oxygen.

If a nitrogen source malfunctions or is set up improperly and nitrogen displaces the existing oxygen in the room containing the printer, a significant hazardous situation may be created. A safety assessment should be performed by your company’s safety officer in order to ensure that your nitrogen system is set up and operated in a safe manner.